Crystal Structure Analysis of Magnetite (Fe3O4) Nanoparticles By Green Synthesis Method Using Moringa Oleifera Extracts

Rizqi A'mal Hibatullah Tabrani, Yudi Guntara, Ganesha Antarnusa, Fazri Firdaus

Abstract


A green synthesis obtained from several basic materials such as FeCl3.6H2O, FeSO4.7H2O, NH4OH, and moringa oleifera extract using the coprecipitation method has been successfully carried out by obtaining Fe3O4 nanoparticle material. Analysis of the crystal structure of Fe3O4 nanoparticles can be seen from the results of characterization using X-Ray Diffraction (XRD) which shows diffraction peaks namely (220), (311), (400), (422), (511), (440), and (533) with the main peak at index (311). The Fe3O4 nanoparticle sample using the natural reducing agent moringa oleifera, was able to eliminate the Fe2O3 diffraction peak and decrease the crystallite size of Fe3O4 nanoparticles. The disappearance of the diffraction peak and the decrease in crystallite size are due to the effect of the addition of moringa oleifera reducing agent which stabilizes during the reaction process.


Keywords


crystal structure, moringa oleifera, nanoparticles Fe3O4

Full Text:

74-80

References


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